Wednesday, November 26, 2025

Chemistry Chapter 20: Electrochemistry

CHEMISTRY KEYWORDS:

Electrolysis: Decomposition of an ionic compound when molten or in aqueous solution by an electric current.

Electrolyte: A molten ionic compound or an aqueous solution of ions that is decomposed during electrolysis.

Electrode: A rod of metal or carbon (graphite) which conducts electricity to or from an electrolyte.

Cathode: Negative electrode (where reduction reactions occur)

Anode: Positive electrode (where oxidation reactions occur).

Faraday: Quantity of electric charge (in coulombs) carried by 1 mole of electrons or 1 mole of singly charged ions.

Electrode Potential, E: Voltage measured for a half-cell compared with another half-cell.

Feasible: Likely to take place. (if E standard has a positive value)

Discharged: Ions changed into atoms or molecules.

 

CHEMISTRY DEFINITIONS:

Standard Electrode Potential: Voltage produced when a standard half-cell (ion concentration 1 mol/dm3 at 298 K) is connected to a standard hydrogen electrode under standard conditions.

Standard Cell Potential: Difference in standard electrode potential between 2 specified half-cells.

 

CHEMISTRY IMPORTANT NOTES:

Electrolysis is a redox reaction. Electrons may be gained or lost in redox reactions.

Species losing electrons is being oxidised and acts as a reducing agent. Oxidation always occurs at the anode (negative terminal of the cell).

Species gaining electrons is being reduced and acts as an oxidising agent. Reduction always occurs at the cathode (positive terminal of the cell).

Electrolysis is often used to extract metals that are high in the reactivity series. It is also used to produce non-metals and to purify some metals. It is generally carried out in an electrolysis cell.

Mass of a substance produced at an electrode during electrolysis is proportional to:

·       Time over which a constant electric current passes.

·       Strength of the electric current.

Mass of a substance produced at an electrode during electrolysis is proportional to the quantity of electricity (in coulombs) which passes through the electrolyte.

Avogadro constant, L, is the number of specified particles in 1 mole.

Redox equilibrium exists between 2 chemically related species that are in different oxidation states. It is established when the rate of electron gain equals the rate of electron loss.

When a metal is placed into a solution of its ions, we establish an electric potential (voltage) between the metal and the metal ions in solution. We can measure the difference in potential between the metal/metal ion system and another system. Electrode potential is measured in volts. The system used for comparison is the standard hydrogen electrode.

The standard hydrogen electrode is one of several types of half-cells used as reference electrodes. Hydrogen gas at 101 kPa, and a concentration of 1.00 mol/ dm3. A platinum electrode covered with platinum black is in contact with hydrogen gas and H+ ions. The platinum electrode is inert, so it does not take part in the reaction.

Electrode potential refers to a reduction reaction. So electrons appear on the left-hand side of the half-equation.

The more positive (or less negative) the electrode potential, the easier it is to reduce the ions on the left. Metal on the right is relatively unreactive and is a poor reducing agent.

The more negative (or less positive) the electrode potential, the more difficult it is to reduce the ions on the left. Metal on the right is relatively reactive and is a good reducing agent.

Standard conditions to make a half-cell:

·       Ions have a concentration of 1.00 mol/dm3.

·       Temperature is 25 °C (298 K).

·       Rod must be pure.

Half-cells are connected using:

·       Wires connected the metal rods in each half-cell to a high-resistance voltmeter. Electrons flow around this external circuit from the metal with the more negative (or less positive) electrode potential to the metal with the less negative (or more positive) electrode potential.

·       Salt bridge to complete the electrical circuit, allowing the movement of ions between the 2 half-cells so that ionic balance is maintained. It does not allow the movement of electrons.

Position of equilibrium of a reaction may be affected by changes in concentration of reagents, temperature and pressure of gases. The voltage of an electrochemical cell will also depend on these factors.

Standard electrode potential is sometimes referred to as standard reduction potential because it refers to the reduction reaction (addition of electrons).

The standard electrode potential for a half-cell is the voltage measured under standard conditions with a standard hydrogen electrode as the other half-cell.

The 3 main types of half-cells can be connected to a standard hydrogen electrode:

·       Metal/metal ion half-cell

·       Non-metal/non-metal ion half-cell

·       Ion/ion half-cell

In half-cells that do not contain a metal, electrical contact with the solution is made by using a platinum wire or platinum foil as an electrode. Platinum must be in contact with both the element and the aqueous solution of its ions.

Standard electrode potential values measure how easy or difficult it is to oxidise/reduce powers of elements and ions by comparing the E standard values for their half-reactions.

·       The more positive the value of E standard, the greater the tendency for the half-equation to proceed in the forward direction. Easier to reduce the species on the left of the half-equation.

·       The less positive the value of E standard, the greater the tendency for the half-equation to proceed in the reverse direction. Easier to oxidise species on the left of the half-equation.

A reaction is feasible if it is likely to occur. If forward reaction is feasible, the reverse reaction is not feasible.

·       Species on the left of the equation become weaker oxidising agents, as they accept electrons less readily.

·       Species on the right of the equation become stronger reducing agents, as they release electrons more readily.

Cations (positive ions) move towards the cathode, where they gain electrons; the gain of electrons is reduction. Anions (negative ions) move towards the anode, where they lose electrons; loss of electrons is oxidation.

SO42- < NO3- < Cl- < OH- < Br- < I- (Increasing ease of discharge, and oxidation)

The proportion of oxygen increases, the more dilute the solution.

 

SUMMARY:

Q = It (Charge = Current x Time)

1 F = 96500 C / mol

F = Le (F = Faraday Constant, L = Avogadro Constant, e = Electron Charge)

L = (charge on 1 mole of electrons) / (1.6 x 10-19 C)

During electrolysis, reduction occurs at the cathode (negative electrode) because ions gain electrons from the cathode, and oxidation occurs at the anode (positive electrode) because ions lose electrons to the anode.

A metal is formed at the cathode and a non-metal at the anode when molten metal salts are electrolysed. Hydrogen may be formed at the cathode and oxygen at the anode when a dilute aqueous solution of metal salts is electrolysed.

A standard hydrogen electrode is a half-cell in which hydrogen gas at a pressure of 101 kPa bubbles through a solution of 1.00 mol/dm3 H+ ions.

The standard electrode potential of a half-cell is the voltage of the half-cell under standard conditions compared with a standard hydrogen electrode.

The direction of electron flow in a simple cell is from the half-cell that has the more negative (or less positive) electrode potential to the half-cell that has the less negative (or more positive) electrode potential.

A particular redox reaction will occur if the E standard of the half-equation involving the species being reduced is more positive than the E standard of the half-equation of the species being oxidised.

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